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    Por favor, use este identificador para citar o enlazar este ítem:http://uvadoc.uva.es/handle/10324/30769

    Título
    Immobilization of lutetium bisphthalocyanine in nanostructured biomimetic sensors using the LbL technique for phenol detection
    Autor
    Rodríguez Méndez, María LuzAutoridad UVA Orcid
    Giuliani, E.
    Saja Saez, José Antonio DeAutoridad UVA Orcid
    Zucolotto, V.
    C. Brazaca, Laís
    Ramos Fernandes, Edson Giuliani
    Año del Documento
    2011
    Descripción
    Producción Científica
    Documento Fuente
    Biosensors and BIoelectronics vol. 26 p. 4715-4719
    Résumé
    This study describes the development of amperometric sensors based on poly(allylamine hydrochloride) (PAH) and lutetium bisphthalocyanine (LuPc2) films assembled using the Layer-by-Layer (LbL) technique. The films have been used as modified electrodes for catechol quantification. Electrochemical measurements have been employed to investigate the catalytic properties of the LuPc2 immobilized in the LbL films. By chronoamperometry, the sensors present excellent sensitivity (20 nA μM−1) in a wide linear range (R2 = 0.994) up to 900 μM and limit of detection (s/n = 3) of 37.5 × 10−8 M for catechol. The sensors have good reproducibility and can be used at least for ten times. The work potential is +0.3 V vs. saturated calomel electrode (SCE). In voltammetry measurements, the calibration curve shows a good linearity (R2 = 0.992) in the range of catechol up to 500 μM with a sensitivity of 90 nA μM−1 and LD of 8 μM.
    ISSN
    0956-5663
    Revisión por pares
    SI
    DOI
    10.1016/j.bios.2011.05.032
    Idioma
    eng
    URI
    http://uvadoc.uva.es/handle/10324/30769
    Derechos
    openAccess
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    • DEP63 - Artículos de revista [331]
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    Attribution-NonCommercial-NoDerivatives 4.0 InternationalExcepté là où spécifié autrement, la license de ce document est décrite en tant que Attribution-NonCommercial-NoDerivatives 4.0 International

    Universidad de Valladolid

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