RT info:eu-repo/semantics/article T1 Phenolic characterization of aging wine lees: correlation with antioxidant activities A1 Romero Díez, Rut A1 Rodríguez Rojo, Soraya A1 Cocero Alonso, María José A1 Duarte, Catarina M.M. A1 Matias, Ana A. A1 Bronze, Maria Rosario K1 Aging wine lees K1 Phenolic Characterization K1 Antioxidant activity K1 LC-MS/MS K1 Correlation study K1 Anthocyanins AB Aging wine lees are water-wastes produced during the wine aging inside wood barrels that can be considered as alternative sources of bioactive compounds. Phenolic characterization and antioxidant activity (AA) measurements of wines lees solid-liquid extracts have been undertaken on a dry extract (DE) basis. Solvents with different polarities (water, methanol, ethanol, two hydroalcoholic mixtures and acetone) were used. Total phenolic (TPC) and total flavonoid contents (TFC) were determined. The mixture of 75:25(v/v) EtOH:H2O showed the highest values with 254mgGAE/gDE and 146mgCATE/gDE respectively. HORAC, HOSC and FRAP were used to determine the AA of the extracts being also highest for the mixture of 75:25(v/v) EtOH:H2O (4,690 µmolCAE/gDE, 4,527 µmolTE/gDE and 2,197 µmolTE/gDE, respectively). For ORAC method, methanol extract showed the best value with 2,771µmolTE /gDE. Correlations between TPC, TFC, phenolic compounds and AA were determined. Most relevant compounds contributing to AA were identified using data from mass spectrometry, being mainly anthocyanins. PB Elsevier Ltd. YR 2018 FD 2018 LK http://uvadoc.uva.es/handle/10324/31433 UL http://uvadoc.uva.es/handle/10324/31433 LA eng NO Food Chemistry, 2018, vol. 259, p.188–195 DS UVaDOC RD 12-jul-2024