RT info:eu-repo/semantics/article T1 Low-frequency ultrasonication modulates the impact of annealing on physicochemical and functional properties of rice flour A1 Vela Corona, Antonio José A1 Villanueva Barrero, Marina A1 Ronda Balbás, María Felicidad K1 Rice flour K1 Low-frequency ultrasound treatment K1 Annealing K1 Thermal properties K1 Gel rheological properties K1 Biopolymers structure K1 3309 Tecnología de Los Alimentos K1 3309.11 Fabricación de Harina AB Ultrasonication (US) is a green technology used to physically modify flours to increase their industrial range of applicability. The aim of this work was to study the combined effect that dual US and annealing (ANN) treatments have on starch and protein structure of rice flour, at 20, 40, 50 and 60 °C. Results showed clear modifications of functional, thermal and pasting properties of flours, as well as rheological properties of gels made from them. US+ANN led to generation of small-size particles, which markedly increased the swelling power and starch damage. X-Ray Diffraction and FTIR indicated that starch crystallinity and protein secondary structure was affected by the shear forces of cavitation. The combination of US+ANN improved the crystalline structure arrangement within the starch granules, causing narrowing of the gelatinization temperature range (ΔT). Pasting viscosities were significantly decreased by ultrasonication, following an increasing trend with increasing temperature, while pasting temperature was increased, agreeing in the achievement of a thermodynamically more stable structure. The rheological properties indicated a reduction of the elastic (G') and viscous (G'') moduli after ultrasonication, as well as lower values of tan (), reflecting a higher predominance of elastic modulus versus viscous one than the non-sonicated flours. The rice flour’s properties were found to be highly sensitive to the applied treatment conditions, showing a synergetic effect when sonicating at the highest studied temperature. PB Elsevier SN 0268-005X YR 2021 FD 2021 LK https://uvadoc.uva.es/handle/10324/49018 UL https://uvadoc.uva.es/handle/10324/49018 LA eng NO Food Hydrocolloids, November 2021, vol. 120, 106933 NO Producción Científica DS UVaDOC RD 22-dic-2024