RT info:eu-repo/semantics/article T1 Phenolic Compounds Extraction of Arbutus unedo L.: Process Intensification by Microwave Pretreatment A1 Alexandre, Agostinho A1 Matias, Ana A. A1 Bronze, Maria Rosario A1 Cocero Alonso, María José A1 Mato Chaín, Rafael Bartolomé K1 Arbutus unedo K1 Phenolic compounds K1 Compuestos fenólicos AB Arbutus unedo L., commonly known as the strawberry-tree fruit, is an endemic species of the Mediterranean flora. Microwave extraction technology has been considered as a fast and “green” method for the production of extracts rich in bioactive compounds, although the energy consumption is high. To overcome this bottleneck, microwave was used as a pretreatment procedure in short time periods. This technique promotes the burst of intracellular vacuoles leading to an increase in the lixiviation of phenolic compounds. Different approaches were tested, namely a solvent-free irradiation (SFI), a solvent-assisted irradiation (SAI) and a pressurized solvent-assisted irradiation (PSAI). After irradiation, a solid–liquid extraction procedure was performed using a mixture of water and ethanol. A kinetic evaluation of the total phenolic content (TPC) was performed using the Folin–Ciocalteu method. For the total anthocyanin content, a UV-spectrophotometric method was used. HPLC-UV and LC-MS were used for TPC and identification of present compounds. Microwave irradiation led to an increase in TPC of extracts after SAI (52%) and PSAI (66%) along with a reduction in time of extraction from 30 min to less than 2 min. The anthocyanin content also increased by 66% for the SAI and PSAI extractions. PB MDPI SN 2227-9717 YR 2020 FD 2020 LK https://uvadoc.uva.es/handle/10324/52455 UL https://uvadoc.uva.es/handle/10324/52455 LA eng NO Processes, 2020, vol. 8, n. 3, 298 NO Producción Científica DS UVaDOC RD 23-nov-2024