RT info:eu-repo/semantics/article T1 Microwave pretreatment for the extraction of anthocyanins from saffron flowers: Assessment of product quality A1 Álvarez Martín, Ana A1 Terreros Calvo, Sara A1 Cocero Alonso, María José A1 Mato Chaín, Rafael Bartolomé K1 Azafrán - Cultivo y producción K1 Antioxidantes K1 Microwaves K1 Microondas K1 Polyphenols K1 Polifenoles K1 Color K1 Saffron flowers K1 Kinetic analysis AB The potential of saffron flowers as a source of polyphenols, and in particular anthocyanins, for the extraction of bioactive compounds and the production of a cyanic colorant was analyzed. A microwave pretreatment, prior to the conventional solid–liquid extraction process, was proposed as a feasible intensification step. The effectiveness of microwave pretreatment was assessed in terms of increased yield and improved quality of the final product. The operational variables studied were the pretreatment temperature (60–120 °C) and the solid–liquid ratio (0.30–0.50 g/mL). It was found that the addition of the microwave pretreatment to the conventional process allowed one to reduce extraction time by up to 12 times and to greatly improve the characteristics of the final product, using microwave energy densities as low as 0.16–0.54 kJ/mL. The extract quality was evaluated in terms of polyphenol richness (25% increase), product composition (80% of the anthocyanins was delphinidin), antioxidant capacity (boosted by the pretreatment) and color (variations in red and blue hue depending on conditions). To conclude, a microwave pretreatment in which the material is heated to a temperature of 65 °C with a solvent ratio of 0.30 g/mL was selected as the optimum to maximize process efficiency and product quality. PB MDPI SN 2076-3921 YR 2021 FD 2021 LK https://uvadoc.uva.es/handle/10324/59336 UL https://uvadoc.uva.es/handle/10324/59336 LA eng NO Antioxidants, 2021, Vol. 10, Nº. 7, 1054 NO Producción Científica DS UVaDOC RD 30-nov-2024