RT info:eu-repo/semantics/article T1 Opportunities for ivory nut residue valorization as a source of nanocellulose colloidal suspensions A1 Carvajal Barriga, Enrique Javier A1 Putaux, Jean-Luc A1 Martín Ramos, Pablo A1 Simbaña, Jennifer A1 Portero Barahona, Patricia A1 Martín Gil, Jesús K1 Polymers K1 Biomaterials K1 Nanocellulose K1 Agricultural engineering K1 Agricultural residues K1 Residuos agrícolas K1 Sustainable development K1 Desarrollo sostenible K1 Palm trees K1 Palmeras K1 Agriculture - Latin America K1 Agricultura - América Latina K1 Forests and forestry K1 Bosques y silvicultura K1 Plant science K1 Chemistry, Organic K1 Ivory nut K1 Nuez de marfil K1 2206.10 Polímeros K1 2304.02 Celulosa K1 3102 Ingeniería Agrícola K1 3106 Ciencia Forestal K1 3106.08 Silvicultura K1 2306 Química Orgánica AB Ivory nut seeds have been traditionally exploited in Central and South America for obtaining vegetable ivory. The residues from this industry are susceptible to valorization as a source of fatty acids (by organic extraction) and mannans (by alkaline dissolution and regeneration). Nonetheless, cellulose may also be recovered at the end of this fractionation process by acid hydrolysis and functionalization, with associated advantages over other lignocellulosic sources due to the absence of lignin in the endospermic tissue. In this work, various experimental parameters (sulfuric acid concentration, temperature, and hydrolysis time) were investigated to optimize the processing conditions for preparing stable nanocellulose suspensions after ultrasonication. The most stable nanocellulose gel (1 wt% solid content) was obtained after 4-h hydrolysis at 60 °C with 8 M H2SO4 and was characterized by using complementary tech-niques, including dynamic light scattering (DLS), transmission electron microscopy (TEM), X-ray powder diffraction (XRD), nano-fibril sulfation measurements, vibrational and solid-state nuclear magnetic resonance (CP/MAS 13C-NMR) spectroscopies, and thermal analysis. This nanocellulose hydrogel is susceptible to further utilization in various applications and fields, e.g., in agricul-ture for controlling the release of agrochemicals, in pharmaceutics for developing new dosage forms, and in the treatment of wastewater from the textile and paper industries. PB MDPI SN 2310-2861 YR 2022 FD 2022 LK https://uvadoc.uva.es/handle/10324/69577 UL https://uvadoc.uva.es/handle/10324/69577 LA eng NO Gels, 2023, Vol. 9, Nº. 1, 32 NO Producción Científica DS UVaDOC RD 18-nov-2024